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Cryogenic ion milling cross-section processing example (rubber products)

Introducing a case study on the method of processing cross-sections using toy car tires!

We would like to introduce a case where cross-sections were created and observed for the adhesive parts of pull-back car tires using different methods. Upon conducting SEM observations of the created cross-sections, fillers present within the rubber were confirmed. It was found that the dispersion state of the fillers and the appearance of the adhesive interface were not clear with liquid nitrogen fracturing or mechanical polishing. In contrast, cross-sections created by cryo ion milling allow for a clear observation of the dispersion state of fillers contained within the rubber and the appearance of the adhesive interface with the plastic substrate. 【Cross-section Preparation Methods】 ■ Liquid Nitrogen Fracturing (-196°C) ■ Mechanical Polishing ■ Cryo CP (-150°C) *For more details, please download the PDF or feel free to contact us.

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Effects of heat generated during cross-sectional ion milling (CP) processing.

We would like to present the results of our observations on the production of cross-sections of rubber products and a comparison of cross-section manufacturing methods!

We will introduce a case study comparing cross-section preparation methods on the surface coating layer of a golf ball and observing the effects of heat from CP processing. There are two layers of coating on the outermost layer of the cover layer, and we conducted a comparison of cross-section preparation methods using this coating layer. SEM observations were performed on cross-sections prepared using three different methods. While cross-section preparation of soft materials is effectively done using cross-section ion milling (CP), the physical properties may change due to the heat generated during CP processing. In such cases, cross-section preparation using cryo-CP, which mitigates the effects of processing heat through cooling, is effective. 【Cross-section Preparation Methods】 ■ Mechanical Polishing ■ CP ■ Cryo-CP (-50°C) *For more details, please download the PDF or feel free to contact us.

  • Measurement and Inspection

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